Mechanical Properties of Individual Southern Pine Fibers. Part I. Determination and Variability of Stress-Strain Curves with Respect to Tree Height and Juvenility

Authors

  • Les Groom
  • Laurence Mott
  • Stephen Shaler

Keywords:

Modulus of elasticity, ultimate tensile stress, juvenility, confocal scanning laser microscope, cross-sectional area, microfibril angle

Abstract

This paper is the first in a three-part series investigating the mechanical properties of loblolly pine fibers. This paper outlines the experimental method and subsequent variation of latewood fiber mechanical properties in relation to tree position. Subsequent papers will deal with differences between earlywood and latewood fibers and effect of juvenility and tree height on global fiber properties. In this paper, the mechanical properties were determined on individual wood fiber with a user-built tensile testing apparatus. Cross-sectional areas of post-tested fibers were determined with a confocal scanning laser microscope and used to convert acquired load-elongation curves into stress-strain curves. The modulus of elasticity and ultimate tensile stress of loblolly pine latewood fibers tested in this study ranged from 6.55 to 27.5 GPa and 410 to 1,422 MPa, respectively. Fibers from the juvenile core of the main stem were on the low end of the mechanical property scale, whereas fibers beyond the twentieth growth ring were near the high end of the scale. Coefficient of variation for fiber stiffness and strength averaged around 20 to 25%. The shape of the fiber stress-strain curves is dependent on their growth ring origins: Mature fibers were linear from initial loading until failure, whereas juvenile fibers demonstrated curvilinearity until about 60% of maximum load followed by linear behavior to failure.

References

Bobalek, J. F., and M. Chaturvedi. 1988. The effect of recycling on the physical properties of specific fibers and their networks. Pages 183-187 in Proc. 1988 TAPPT. Pulping Conference. Book 1.nCave, I. D. 1969. The longitudinal Youngs modulus of Pinus radiata.Wood Sci. Technol.3(1):40-48.nDuncker, B., and L. Nordman. 1965. Determination of strength of single fibers. Paperi Jaa Puu10:539-552.nEhrnrooth, E. M. L., and P. Kolseth. 1984. The tensile testing of single wood pulp fibers in air and in water. Wood Fiber Sci.16(4):549-566.nEl-Hosseiny, F., and D. H. Page. 1975. The mechanical properties of single wood pulp fibers. II—Theories of strength. Fiber Sci. Technol.8:21.nGroom, L. H., S. M. Shaler, and L. Mott. 1995. Characterizing micro- and macromechanical properties of single wood fibers. Pages 13-18 in 1995 International Paper Physics Conference, September 11-14, 1995, Niagara-on-the-Lake, Ontario.nGroom, L. H., S. M. Shaler, and L. Mott. 1996. Physical and mechanical properties of virgin and recycled wood fibers. Pages 20-35 in Proc., Forest Products Society Southeast Section Annual Meeting November 11-12, 1994, Atlanta, GA.nHardacker, K. W. 1963. The automatic recording of the load-elongation characteristics of single papermaking fibers. Tappi45(3):237-246.nHartler N., G. Kull, and L. Stockman. 1963. Determination of fiber strength through measurement of individual fibers. Sven. Papperstidn.66(8):301-311.nJang, H. F., A. G. Robertson, and R. S. Seth. 1991. Optical sectioning of pulp fibers with confocal scanning laser microscopy. Pages 277-280 in Tappi Proc. 1991 International Paper Physics Conference.nJayne, B. A. 1959. Mechanical properties of wood fibers. Tappi42(6):461-467.nJayne, B. A. 1960. Wood fibers in tension. Forest Prod. J.10(6):316-322.nJones, G. L. 1989a. Stimulating end use performance. Tappi72(10):189-197.nJones, G. L. 1989b. Strategies for end use performance. in Proc. Contaminant Problems and Strategies in Waste-paper Recycling. Tappi Press. 1989.nKaldor, A. F. 1992. Kenaf, an alternative fiber for the pulp and paper industries in developing and developed countries. Tappi75(10):141-145.nKellogg, R. M., and F. Wangaard. 1964. Influence of fiber strength on sheet properties of hardwood pulps. Tappi47(6):361-367.nKersavage, P. C. 1973. A system for automatically recording the load-elongation characteristics of single wood fibers under controlled relative humidity conditions. USDA. U.S. Government Printing Office. 46 pp.nKim, C. Y., D. H. Page, F. El-Hosseiny, and A. P. Lancaster. 1975. The mechanical properties of single wood pulp fibers. Part 3: The effects of drying on strength. J. Appl. Polymer Sci.19(8):1549-1561.nKlauditz, W., Marshchall, A., and W. Ginzel. 1947. Zur technologie verholtzer pflanzlicher zellwande. Holzforschung1(4):98-103.nKlungness, J. H. 1974. Recycled fiber properties as affected by contaminants and removal processes. USDA. U.S. Government Printing Office. 16 pp.nLeopold, B., and D. C. McIntosh. 1961. Chemical composition and physical properties of wood fibers. Tappi44(3):235-240.nLeopold, B., and J. L. Thorpe. 1968. Effect of pulping on strength properties of dry and wet pulp fibers from Norway spruce. Tappi51(7):304-308.nLuner, P., K. P. Vemuri, and F. Womeldorf. 1967. The effect of chemical modification on the mechanical properties of paper. III. Dry strength of oxidized springwood and summerwood southern pine kraft fibers. Tappi50(5):227-230.nMcIntosh, D. C. 1963. Tensile strength of loblolly pine fibers cooked to different yields. Tappi46(5):237-277.nMcIntosh, D. C., and L. O. Uhrig. 1968. Effect of refining on load-elongation characteristics of loblolly pine holocellulose and unbleached Kraft fibers. Tappi51(6):268-273.nMcKee, R. C. 1971. Effect of repulping on sheet properties and fiber characteristics. Paper Trade J.155(21): 34-40.nMcMillan, C. W. 1968. Morphological characteristics of loblolly pine wood as related to specific gravity, growth rate, and distance from pith. Wood Sci. Technol.2:166-176.nMegraw, R. A. 1985. Wood quality factors in Loblolly Pine. Tappi Press, Atlanta, GA.nMegraw, R. A., D. Bremer, G. Leaf, and J. Roers. 1999. Stiffness in loblolly as a function of ring position and height, and its relationship to microfibril angle and specific gravity. Pages 341-349 in Proc. Third Workshop: Connection Between Silviculture and Wood Quality through Modeling Approaches and Simulation Software. IUFRO working party S5.01-04, September 5-12 La Londe-Les-Maures, France.nMott, L. 1995. Micromechanical properties and fracture mechanisms of single wood pulp fibers. Ph.D. dissertation, University of Maine, Orono, Maine. 198 pp.nMott, L., S. M. Shaler, and L. H. Groom. 1996. A technique to measure strain distributions in single wood pulp fibers. Wood Fiber Sci.28(4):429-437.nOye, R. 1985. Degradation of pulp fibers by recycling. Pages 109-110 in Proc. ISF-85. August 20-24, 1985, Hakone, Japan. Vol. 3.nPage, D. H., and F. El-Hosseiny. 1976. The mechanical properties of single wood pulpfibers. Part 4: The influence of defects. Sven. Papperstidn.14:471-474.nPage, D. H., F. El-Hosseiny, and K. Winkler. 1971. Behaviour of single wood fibres under axial tensile strain. Nature. 229 (5282):252-253.nPage, D. H., F. El-Hosseiny, K. Winkler and R. Bain. 1972. The mechanical properties of single wood pulp fibers. Part 1: A new approach. Pulp Paper Mag. Canada73(8):72-76.nPage, D. H., F. El-Hosseiny, K. Winkler and A. P. Lancaster. 1977. Elastic modulus of single wood pulp fibers. Tappi60(4): 114-117.nPycraft. C. J. H., and P. Howarth. 1980. Does better paper mean worse waste paper? Pap. Technol. Ind.21(10):321-324.nShaler, S. M., L. H. Groom, and L. Mott. 1996. Microscopic analysis of wood fibers using ESEM and confocal microscopy. Pages 25-32 in Woodfiber/Plastic Composites: Virgin and Recycled Wood Fiber and Polymers for Composites, Proc. No. 7293, May 1-3, 1995. Madison, WI.nTamolang, F. N., F. F. Wangaard, and R. M. Kellogg. 1967. Strength and stiffness of hardwood fibers. Tappi50(2):68-71.nVan den Akker, J. A. 1970. Fibril angle for maximum tensile strength of a cross-linked helical structure of fibrils. D. H. Page, ed. in The physics and chemistry of wood pulp fibres, Special Technical Association Publication No. 8, Tappi, New York, NY.nVan den Akker, J. A., A. L. Lathrop, M. Voelker, and M. Dearth. 1958. Importance of fiber strength to sheet strength. Tappi41(8):416-425.nVan Wyk, W., and G. Gerischer. 1982. The influence of recycling on the strength properties of machine made paper. Paperi ja Puu.9:526-533.n

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2007-06-05

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