Revealing Fibril Angle in Wood Sections By Ultrasonic Treatment
Keywords:
Cell-wall checking, Congo Red, fibril angle, southern pine, ultrasoundAbstract
An effective method for inducing cell-wall checks in a microtomed wood radial section by ultrasonic treatment is described. Congo Red enhances cell-wall fibrillation in ultrasonic-treated sections. The amount of fibrillation and checking increases as ultrasonic treatment continues. However, too much fibrillation generated either by prolonged ultrasonic treatment or by Congo Red enhancement may visually obscure the checks. Less than three hours of ultrasonic treatment at 47 kHz frequency was found to be satisfactory to induce checks in 15-μm-thick southern pine sections. The ultrasound check-inducing technique is most effective on southern pine fibers with large diameters and high fibril angles.References
Boyd, J. D. 1973. Appraising methods of measuring microfibril angles. Wood Science 6(1):95-96.nCracknell, A. P. 1980. Ultrasound as a form of energy in industry and medicine. In Ultrasonic. Crane, Russak & Co., New York, NY.nCrgsby, C. M., and R. E. Mark. 1974. Precise S2 angle determination in pulp fibers. Svensk Papperstidn. 17:636-642.nInstitute of Paper Chemistry. 1972. Effect of ultrasonics on fibers and pulp, an annotated bibliography. Institute of Paper Chemistry S56. Appleton, WI.nIwasaki, T., B. Lindberg, and H. Meier. 1962. The effect of ultrasonic treatment on individual wood fibers. Svensk Papperstidn. 65:795-816.nLaine, J. E., J. M. MacLeod, H. I. Bolker, and D. A. I. Goring. 1976. Application of ultrasound in pulp and paper technology. Pulp Paper Res. Inst. Can. PPR No. 148.nLaine, J. E., T. Sloan, and G. G. Allan. 1980. Modification of the refining process by additives, particularly Congo Red. Pages 237-251 in International symposium on fundamental concepts of refining. Appleton, WI.nMacIntosh, D. C. 1967. The effect of refining on the structure of the cell wall. Tappi 50(10):482-488.nMark, H. F., N. M. Bikales, C. G. Overberger, and G. Menges. 1986. Dyeing. Page 233 in Encyclopedia of polymer science and engineering., 2nd ed., vol. 5. John Wiley & Sons, New York, NY.nMark, R. E., and P. P. Gillis. 1973. The relationship between fiber modulus and S2 angle. Tappi 56(4):164-167.nMarts, R. O. 1955. Fluorescence microscopy for measuring fibril angles in pine tracheids. Stain Technol. 30(5):243-248.nMegraw, R. A. 1985. Fibril angle. Pages 49-62 in Wood quality factors in loblolly pine. Tappi Press.nMeylan, B. A. 1967. Measurement of microfibril angle by X-ray diffraction. Forest Prod. J. 17(5):51-58.nMiniutti, V. P. 1964. Microscale changes in cell structure at softwood surfaces during weathering. Forest Prod. J. 14(12):571-576.nMohlin, U-B., and O. Lidbrandt. 1980. Changes in fiber structure due to refining as revealed by SEM. Pages 61-74 in International symposium on fundamental concepts of refining. Appleton, WI.nPage, D. H., and J. H. De Grace. 1967. Delamination of fiber walls by beating and refining. Tappi 50(10):489-495.nSenft, J. F., and B. A. Bendtsen. 1985. Measuring microfibrillar angles using light microscopy. Wood Fiber Sci. 17(4):564-567.n
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